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Elimination technique for alkali metal ion adducts from an electrospray ionization process using an on-line ion suppressor
http://hdl.handle.net/10112/7433
http://hdl.handle.net/10112/743330531b6a-21b4-4f5d-bed5-70471b906d10
名前 / ファイル | ライセンス | アクション |
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KU-1100-20100610-07.pdf (567.8 kB)
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Item type | 学術雑誌論文 / Journal Article(1) | |||||
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公開日 | 2012-12-10 | |||||
タイトル | ||||||
タイトル | Elimination technique for alkali metal ion adducts from an electrospray ionization process using an on-line ion suppressor | |||||
言語 | ||||||
言語 | eng | |||||
資源タイプ | ||||||
資源タイプ識別子 | http://purl.org/coar/resource_type/c_6501 | |||||
資源タイプ | journal article | |||||
著者 |
Nozaki, Kazuyoshi
× Nozaki, Kazuyoshi× Tarui, Akira× Osaka, Issey× Kawasaki, Hideya× Arakawa, Ryuichi |
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著者別名 | ||||||
姓名 | 野崎, 和吉 | |||||
著者別名 | ||||||
姓名 | 樽井, 章 | |||||
著者別名 | ||||||
姓名 | 大坂, 一生 | |||||
著者別名 | ||||||
姓名 | 川崎, 英也 | |||||
著者別名 | ||||||
姓名 | 荒川, 隆一 | |||||
概要 | ||||||
内容記述タイプ | Other | |||||
内容記述 | The effects of an on-line ion suppressor device on alkali metal ion adduct formations of the model compound tacrolimus were investigated. The base peak ion in the positive ion ESI-MS spectrum of tacrolimus was a sodium ion adduct, [M+Na]+. On the other hand, an ammonium ion adduct, [M+NH4]+, was the base peak ion in the full-scan mass spectrum of tacrolimus with a cation-exchange suppressor resin, and both [M+Na]+ and [M+K]+ were eliminated. These results indicate that the combination of an on-line ion suppressor with ESI-MS is a simple and effective technique that eliminates undesirable alkali metal ion adduct formations in the positive-ion mode. | |||||
書誌情報 |
Analytical Sciences 巻 26, 号 6, p. 715-718, 発行日 2010-06-10 |
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ISSN | ||||||
収録物識別子タイプ | ISSN | |||||
収録物識別子 | 09106340 | |||||
書誌レコードID | ||||||
収録物識別子タイプ | NCID | |||||
収録物識別子 | AA10500785 | |||||
DOI | ||||||
関連タイプ | isIdenticalTo | |||||
識別子タイプ | DOI | |||||
関連識別子 | 10.2116/analsci.26.715 | |||||
著者版フラグ | ||||||
出版タイプ | VoR | |||||
出版タイプResource | http://purl.org/coar/version/c_970fb48d4fbd8a85 | |||||
出版者 | ||||||
出版者 | The Japan Society for Analytical Chemistry | |||||
出版者(他言語) | ||||||
日本分析化学会 |