{"created":"2023-05-15T12:12:52.924452+00:00","id":807,"links":{},"metadata":{"_buckets":{"deposit":"a9f6f4f3-e766-4b2d-bda7-89e4a3838832"},"_deposit":{"created_by":1,"id":"807","owners":[1],"pid":{"revision_id":0,"type":"depid","value":"807"},"status":"published"},"_oai":{"id":"oai:kansai-u.repo.nii.ac.jp:00000807","sets":["85:92:102:1816:104"]},"author_link":["2298","2299","2300","2301","2302","2303"],"control_number":"807","item_10_alternative_title_20":{"attribute_name":"その他のタイトル","attribute_value_mlt":[{"subitem_alternative_title":"Characterization of Organic Binding Media Used in Egyptian Painting Layers by GC/MS","subitem_alternative_title_language":"en"}]},"item_10_biblio_info_7":{"attribute_name":"書誌情報","attribute_value_mlt":[{"bibliographicIssueDates":{"bibliographicIssueDate":"2011-03-08","bibliographicIssueDateType":"Issued"},"bibliographicPageEnd":"109","bibliographicPageStart":"103","bibliographicVolumeNumber":"2","bibliographic_titles":[{"bibliographic_title":"Semawy menu","bibliographic_titleLang":"en"}]}]},"item_10_description_4":{"attribute_name":"概要","attribute_value_mlt":[{"subitem_description":"ガスクロマトグラフィー質量分析（GC-MS）の3種類の測定手法、ダブルショット法、反応熱分解法および液体注入法を用いて、エジプト壁画に使用されている接着剤などの有機化合物の分析を行った。試料はサッカラのイドゥートの埋葬室から得られた壁画の小片である。ダブルショット法、液体注入法を用いたGC-MS測定では、天然物由来の有機化合物を検出することができなかった。反応熱分解法を用いて壁画表面をGC-MSで分析した結果、飽和脂肪酸エステル類が強く、他にも脂肪酸グリセリド様と思われる化合物を検出した。その結果は、前回測定したツナ・エル・ガバル遺跡の壁画小片から検出した有機物とほぼ同じ化合物群であり、今回も壁画に使用されている接着材の成分を識別することはできなかった。3種類の分析方法の中で反応熱分解法が、有機化合物に対してもっとも感度が高かった。","subitem_description_language":"ja","subitem_description_type":"Other"},{"subitem_description":"Organic binding media used in Egyptian wall paintings was characterized using gas chromatograph-mass spectrometry (GC-MS). Samples of the wall paintings were obtained from the dubris in the mastaba of Idout, Saqqara in Egypt. The aim of this study is to investigate the possibility of discrimination between arabic gum and animal protein-based binders used in ancient Egypt. In this present study, three methods of sample preparation and injection in GC-MS (double-shot injection, reaction pyrolysis and liquid-injection) were tested for the most sensitive detection of the organic binding media. The GC-MS results showed that the double-shot injection and liquid-injection methods detected no natural products, but the reaction pyrolysis method could detect saturated fatty-acid esters and fatty-acid glyceride-like compounds. However, these organic compounds found at the Idout wall painting are almost consistent\n with the previously reported compounds that were detected from the wall painting samples obtained from the Funeral House in Tuna el-Gabal. In conclusion, the organic binding media could not be discriminated again.","subitem_description_language":"en","subitem_description_type":"Other"}]},"item_10_identifier_registration":{"attribute_name":"ID登録","attribute_value_mlt":[{"subitem_identifier_reg_text":"10.32286/0000000807","subitem_identifier_reg_type":"JaLC"}]},"item_10_publisher_34":{"attribute_name":"出版者","attribute_value_mlt":[{"subitem_publisher":"関西大学文化財保存修復研究拠点","subitem_publisher_language":"ja"},{"subitem_publisher":"Institute for Conservation and Restoration of Cultural Properties, Kansai University","subitem_publisher_language":"en"}]},"item_10_source_id_10":{"attribute_name":"書誌レコードID","attribute_value_mlt":[{"subitem_source_identifier":"AA12563866","subitem_source_identifier_type":"NCID"}]},"item_10_version_type_17":{"attribute_name":"著者版フラグ","attribute_value_mlt":[{"subitem_version_resource":"http://purl.org/coar/version/c_970fb48d4fbd8a85","subitem_version_type":"VoR"}]},"item_access_right":{"attribute_name":"アクセス権","attribute_value_mlt":[{"subitem_access_right":"open access","subitem_access_right_uri":"http://purl.org/coar/access_right/c_abf2"}]},"item_creator":{"attribute_name":"著者","attribute_type":"creator","attribute_value_mlt":[{"creatorNames":[{"creatorName":"久富, 広隆","creatorNameLang":"ja"},{"creatorName":"Hisatomi, Hirotaka","creatorNameLang":"en"}],"nameIdentifiers":[{}]},{"creatorNames":[{"creatorName":"浅井, 重博","creatorNameLang":"ja"},{"creatorName":"Asai, Shigehiro","creatorNameLang":"en"}],"nameIdentifiers":[{}]},{"creatorNames":[{"creatorName":"川﨑, 英也","creatorNameLang":"ja"},{"creatorName":"Kawasaki, Hideya","creatorNameLang":"en"}],"nameIdentifiers":[{},{}]},{"creatorNames":[{"creatorName":"アフメド・シュエイブ","creatorNameLang":"ja"},{"creatorName":"Ahmed Sayed Shoeib","creatorNameLang":"en"}],"nameIdentifiers":[{}]},{"creatorNames":[{"creatorName":"吹田, 浩","creatorNameLang":"ja"},{"creatorName":"Suita, Hiroshi","creatorNameLang":"en"}],"nameIdentifiers":[{},{}]},{"creatorNames":[{"creatorName":"荒川, 隆一","creatorNameLang":"ja"},{"creatorName":"Arakawa, Ryuichi","creatorNameLang":"en"}],"nameIdentifiers":[{}]}]},"item_files":{"attribute_name":"ファイル情報","attribute_type":"file","attribute_value_mlt":[{"accessrole":"open_date","date":[{"dateType":"Available","dateValue":"2019-05-20"}],"displaytype":"detail","filename":"KU-1100-20110308-10.pdf","filesize":[{"value":"720 KB"}],"format":"application/pdf","licensetype":"license_note","mimetype":"application/pdf","url":{"label":"KU-1100-20110308-10.pdf","objectType":"fulltext","url":"https://kansai-u.repo.nii.ac.jp/record/807/files/KU-1100-20110308-10.pdf"},"version_id":"5a0b1588-c267-4f76-bc63-a90a9dfeb647"}]},"item_keyword":{"attribute_name":"キーワード","attribute_value_mlt":[{"subitem_subject":"エジプト","subitem_subject_language":"ja","subitem_subject_scheme":"Other"},{"subitem_subject":"サッカラ","subitem_subject_language":"ja","subitem_subject_scheme":"Other"},{"subitem_subject":"文化財","subitem_subject_language":"ja","subitem_subject_scheme":"Other"},{"subitem_subject":"修復","subitem_subject_language":"ja","subitem_subject_scheme":"Other"},{"subitem_subject":"関西大学","subitem_subject_language":"ja","subitem_subject_scheme":"Other"},{"subitem_subject":"Kansai University","subitem_subject_language":"en","subitem_subject_scheme":"Other"}]},"item_language":{"attribute_name":"言語","attribute_value_mlt":[{"subitem_language":"jpn"}]},"item_resource_type":{"attribute_name":"資源タイプ","attribute_value_mlt":[{"resourcetype":"departmental bulletin paper","resourceuri":"http://purl.org/coar/resource_type/c_6501"}]},"item_title":"ガスクロマトグラフィー質量分析による壁画中の有機化合物の分析","item_titles":{"attribute_name":"タイトル","attribute_value_mlt":[{"subitem_title":"ガスクロマトグラフィー質量分析による壁画中の有機化合物の分析","subitem_title_language":"ja"}]},"item_type_id":"10","owner":"1","path":["104"],"pubdate":{"attribute_name":"PubDate","attribute_value":"2012-01-26"},"publish_date":"2012-01-26","publish_status":"0","recid":"807","relation_version_is_last":true,"title":["ガスクロマトグラフィー質量分析による壁画中の有機化合物の分析"],"weko_creator_id":"1","weko_shared_id":-1},"updated":"2023-10-11T06:47:37.503805+00:00"}