{"created":"2023-05-15T12:20:53.525341+00:00","id":11608,"links":{},"metadata":{"_buckets":{"deposit":"d005a438-01f0-44a5-a1df-8911b014ecd7"},"_deposit":{"created_by":1,"id":"11608","owners":[1],"pid":{"revision_id":0,"type":"depid","value":"11608"},"status":"published"},"_oai":{"id":"oai:kansai-u.repo.nii.ac.jp:00011608","sets":["528:1588:1595:1597"]},"author_link":["27577","27581","27583","27582","27584","27578","27576","27580","27585","27579"],"item_9_alternative_title_20":{"attribute_name":"その他のタイトル","attribute_value_mlt":[{"subitem_alternative_title":"Analysis of Contaminants Eluted from Vials, Septa and Syringe Filters in High-Performance Liquid Chromatography/Mass Spectrometry"}]},"item_9_biblio_info_7":{"attribute_name":"書誌情報","attribute_value_mlt":[{"bibliographicIssueDates":{"bibliographicIssueDate":"2009-02-05","bibliographicIssueDateType":"Issued"},"bibliographicIssueNumber":"2","bibliographicPageEnd":"100","bibliographicPageStart":"95","bibliographicVolumeNumber":"58","bibliographic_titles":[{"bibliographic_title":"分析化学"}]}]},"item_9_description_4":{"attribute_name":"概要","attribute_value_mlt":[{"subitem_description":"高速液体クロマトグラフィー/質量分析法(LC/MS)を用いて分析を行う際に,様々な汚染物質のイオンが検出される場合がある.このことは,LC/MSの高精度な定性・定量分析を困難にする.汚染物質の混入を防ぐには,汚染物質の同定とそのイオンの出所を知っておく必要がある.今回,著者らはLC/MSで使用するバイアルとセプタム,そして炉過用膜フィルターに着目した.LC/MS及びMS^n分析により,幾つかの汚染物質を同定し,その原因を特定した.\nVarious contaminants might be frequently detected in high-performance liquid chromatography/mass spectrometry (LC/MS) experiments. This makes highly accurate qualitative and quantitative analyses of LC/MS difficult. It is necessary to know the identification and origin of the contaminants to prevent them from being mixed. In the present work, we paid attention to any contaminants eluted from vials, septa and syringe filters used for an automatic sampling device and filtration preparation in LC/MS experiments. Some contaminants were identified by LC/MS and MS/MS analysis. In addition, we could specify the contaminant source.","subitem_description_type":"Other"}]},"item_9_full_name_3":{"attribute_name":"著者別名","attribute_value_mlt":[{"nameIdentifiers":[{"nameIdentifier":"27581","nameIdentifierScheme":"WEKO"}],"names":[{"name":"Yoshimoto, Arifumi"}]},{"nameIdentifiers":[{"nameIdentifier":"27582","nameIdentifierScheme":"WEKO"}],"names":[{"name":"Nishimoto, Yukari"}]},{"nameIdentifiers":[{"nameIdentifier":"27583","nameIdentifierScheme":"WEKO"}],"names":[{"name":"Ishihara, Chizuko"}]},{"nameIdentifiers":[{"nameIdentifier":"27584","nameIdentifierScheme":"WEKO"}],"names":[{"name":"Kawasaki, Hideya"}]},{"nameIdentifiers":[{"nameIdentifier":"27585","nameIdentifierScheme":"WEKO"}],"names":[{"name":"Arakawa, Ryuichi"}]}]},"item_9_publisher_34":{"attribute_name":"出版者","attribute_value_mlt":[{"subitem_publisher":"日本分析化学会"}]},"item_9_source_id_10":{"attribute_name":"書誌レコードID","attribute_value_mlt":[{"subitem_source_identifier":"AN00222633","subitem_source_identifier_type":"NCID"}]},"item_9_source_id_8":{"attribute_name":"ISSN","attribute_value_mlt":[{"subitem_source_identifier":"05251931","subitem_source_identifier_type":"ISSN"}]},"item_9_version_type_17":{"attribute_name":"著者版フラグ","attribute_value_mlt":[{"subitem_version_resource":"http://purl.org/coar/version/c_970fb48d4fbd8a85","subitem_version_type":"VoR"}]},"item_creator":{"attribute_name":"著者","attribute_type":"creator","attribute_value_mlt":[{"creatorNames":[{"creatorName":"芳本, 有史"}],"nameIdentifiers":[{}]},{"creatorNames":[{"creatorName":"西本, ゆかり"}],"nameIdentifiers":[{}]},{"creatorNames":[{"creatorName":"石原, 千津子"}],"nameIdentifiers":[{}]},{"creatorNames":[{"creatorName":"川崎, 英也"}],"nameIdentifiers":[{},{}]},{"creatorNames":[{"creatorName":"荒川, 隆一"}],"nameIdentifiers":[{}]}]},"item_files":{"attribute_name":"ファイル情報","attribute_type":"file","attribute_value_mlt":[{"accessrole":"open_date","date":[{"dateType":"Available","dateValue":"2019-05-23"}],"displaytype":"detail","filename":"KU-1100-20090225-05.pdf","filesize":[{"value":"837.9 kB"}],"format":"application/pdf","licensetype":"license_note","mimetype":"application/pdf","url":{"label":"KU-1100-20090225-05.pdf","url":"https://kansai-u.repo.nii.ac.jp/record/11608/files/KU-1100-20090225-05.pdf"},"version_id":"5b8be1f3-7521-4cb7-b53e-3b7bbb74572e"}]},"item_language":{"attribute_name":"言語","attribute_value_mlt":[{"subitem_language":"jpn"}]},"item_resource_type":{"attribute_name":"資源タイプ","attribute_value_mlt":[{"resourcetype":"journal article","resourceuri":"http://purl.org/coar/resource_type/c_6501"}]},"item_title":"高速液体クロマトグラフィー/質量分析法で使用する器具からの汚染物質の分析","item_titles":{"attribute_name":"タイトル","attribute_value_mlt":[{"subitem_title":"高速液体クロマトグラフィー/質量分析法で使用する器具からの汚染物質の分析"}]},"item_type_id":"9","owner":"1","path":["1597"],"pubdate":{"attribute_name":"公開日","attribute_value":"2012-01-26"},"publish_date":"2012-01-26","publish_status":"0","recid":"11608","relation_version_is_last":true,"title":["高速液体クロマトグラフィー/質量分析法で使用する器具からの汚染物質の分析"],"weko_creator_id":"1","weko_shared_id":1},"updated":"2023-05-15T14:40:37.208980+00:00"}