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ESIおよびFABマススペクトロメトリーを用いるアミン類およびジペプチド類のエナンチオマー過剰度の決定
http://hdl.handle.net/10112/6064
http://hdl.handle.net/10112/606418a8a78e-9be1-4e26-b986-95044524476e
名前 / ファイル | ライセンス | アクション |
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KU-1100-20041001-01.pdf (244.7 kB)
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Item type | 学術雑誌論文 / Journal Article(1) | |||||
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公開日 | 2012-02-21 | |||||
タイトル | ||||||
タイトル | ESIおよびFABマススペクトロメトリーを用いるアミン類およびジペプチド類のエナンチオマー過剰度の決定 | |||||
言語 | ||||||
言語 | jpn | |||||
資源タイプ | ||||||
資源タイプ識別子 | http://purl.org/coar/resource_type/c_6501 | |||||
資源タイプ | journal article | |||||
その他のタイトル | ||||||
その他のタイトル | Enantiomer Excess Determination of Amines and Dipeptides by ESI and FAB Mass Spectrometry Coupled with the Enantiomer-Labeled Host Method | |||||
著者 |
亀井, 亮宏
× 亀井, 亮宏× 荒川, 隆一× 澤田, 正寛× 上野, 弘高× 山田, 等× 高井, 嘉雄× 靜間, 基博× 山岡, 寛史× 田中, 寿一 |
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著者別名 | ||||||
姓名 | Kamei, Akihiro | |||||
著者別名 | ||||||
姓名 | Arakawa, Ryuichi | |||||
著者別名 | ||||||
姓名 | Sawada, Masaki | |||||
著者別名 | ||||||
姓名 | Ueno, Hirotaka | |||||
著者別名 | ||||||
姓名 | Yamada, Hitoshi | |||||
著者別名 | ||||||
姓名 | Takai, Yoshio | |||||
著者別名 | ||||||
姓名 | Shizuyama, Motohiro | |||||
著者別名 | ||||||
姓名 | Yamaoka, Hiroshi | |||||
著者別名 | ||||||
姓名 | Tanaka, Juichi | |||||
概要 | ||||||
内容記述タイプ | Other | |||||
内容記述 | The enantiomeric excess (e.e.) determination of organic amines and dipeptides has been examined using ESI and FAB mass spectrometry. Here, an equimolar amount of labeled and unlabeled enantiomeric host pair compounds is mixed with a given e.e.-unknown guest compound. This is called the enantiomer labeled (EL)-host method. The enantiomeric host pairs employed were (1) chiral podands having galactose end-groups and (2) chiral crown ethers. Three sets of the Ie (intensity excess)-e.e. plot showed excellent linear relationships, indicating that the e.e.-value of e.e.-unknown amine compounds can be determined by the simple ESIMS or FABMS coupled with the EL-host method, within the mean error of 1.5-4%e.e. | |||||
書誌情報 |
Journal of the Mass Spectrometry Society of Japan 巻 52, 号 5, p. 289-294, 発行日 2004 |
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ISSN | ||||||
収録物識別子タイプ | ISSN | |||||
収録物識別子 | 13408097 | |||||
書誌レコードID | ||||||
収録物識別子タイプ | NCID | |||||
収録物識別子 | AA1254271X | |||||
著者版フラグ | ||||||
出版タイプ | VoR | |||||
出版タイプResource | http://purl.org/coar/version/c_970fb48d4fbd8a85 | |||||
出版者 | ||||||
出版者 | Mass Spectrometry Society of Japan | |||||
出版者(他言語) | ||||||
日本質量分析学会 |